@conference{
author = "Lazić, Sanja and Šunjka, Dragana and Grahovac, Nada and Guzsvany, Valéria",
year = "2013",
abstract = "In this paper we have developed an analytical method for the fast determination of acetamiprid
residue in sweet cherry samples. The experiment was carried out using blank
extracted
spiked with a solution of acetamipid insecticide at three levels. This analyte was
preparation
with acetonitrile from fortified sweet cherry samples using QUEChERS sample
HPLC/DAD
procedure. Insecticide determination and quantification were performed by
x 4.6 mm
using reversed phase procedure utilized an Agilent Zorbax Cj cartridge (50 mm internal diameter. 1.8 lum particle size). Mobile phase was acetonitrile/1.5%
correlation
CH3COOH solution. Acetamiprid showed linear calibrations from 0.05—2.5 ug/ml with
mg/kg.
coefficients of 0.995%. Limit of quantification (LOQ) were established as 0.014
the peak
Precision values expressed as relative standard deviation of the retention times and of
ranged 80-94%.
areas were 0.16 and 1.29%, respectively. Recoveries of the acetamiprid were in the
analysis
The proposed method is rapid, simple and could be utilized for the routine of acetamiprid residues in sweet cherry samples.",
publisher = "SZAB Kémiai Szakbizottsag Analitikai és Koernyezetvédelmi Munkabizottsaga",
journal = "Proceedings, 19th International Symposium on Analytical and Environmental Problems, 23 September 2013, Szeged, Hungary",
title = "Determination of acetamiprid residues in sweet cherry samples.",
pages = "59-56",
url = "https://hdl.handle.net/21.15107/rcub_fiver_3303"
}