Determination of acetamiprid residues in sweet cherry samples.
Конференцијски прилог (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
In this paper we have developed an analytical method for the fast determination of acetamiprid
residue in sweet cherry samples. The experiment was carried out using blank
extracted
spiked with a solution of acetamipid insecticide at three levels. This analyte was
preparation
with acetonitrile from fortified sweet cherry samples using QUEChERS sample
HPLC/DAD
procedure. Insecticide determination and quantification were performed by
x 4.6 mm
using reversed phase procedure utilized an Agilent Zorbax Cj cartridge (50 mm internal diameter. 1.8 lum particle size). Mobile phase was acetonitrile/1.5%
correlation
CH3COOH solution. Acetamiprid showed linear calibrations from 0.05—2.5 ug/ml with
mg/kg.
coefficients of 0.995%. Limit of quantification (LOQ) were established as 0.014
the peak
Precision values expressed as relative standard deviation of the retention times and of
ranged 80-94%.
areas were 0.16 and 1.29%, respectively. Recoveries of the acetamiprid were in the
analy...sis
The proposed method is rapid, simple and could be utilized for the routine of acetamiprid residues in sweet cherry samples.
Кључне речи:
acetamiprid / residues / sweet cherry / insecticidesИзвор:
Proceedings, 19th International Symposium on Analytical and Environmental Problems, 23 September 2013, Szeged, Hungary, 2013, 56-59Издавач:
- SZAB Kémiai Szakbizottsag Analitikai és Koernyezetvédelmi Munkabizottsaga
Финансирање / пројекти:
- Стварање слабобујних подлога за трешњу и вишњу и развијање интензивне технологије гајења на принципима одрживе пољопривреде (RS-MESTD-Technological Development (TD or TR)-31038)
Колекције
Институција/група
FiVeRTY - CONF AU - Lazić, Sanja AU - Šunjka, Dragana AU - Grahovac, Nada AU - Guzsvany, Valéria PY - 2013 UR - http://fiver.ifvcns.rs/handle/123456789/3303 AB - In this paper we have developed an analytical method for the fast determination of acetamiprid residue in sweet cherry samples. The experiment was carried out using blank extracted spiked with a solution of acetamipid insecticide at three levels. This analyte was preparation with acetonitrile from fortified sweet cherry samples using QUEChERS sample HPLC/DAD procedure. Insecticide determination and quantification were performed by x 4.6 mm using reversed phase procedure utilized an Agilent Zorbax Cj cartridge (50 mm internal diameter. 1.8 lum particle size). Mobile phase was acetonitrile/1.5% correlation CH3COOH solution. Acetamiprid showed linear calibrations from 0.05—2.5 ug/ml with mg/kg. coefficients of 0.995%. Limit of quantification (LOQ) were established as 0.014 the peak Precision values expressed as relative standard deviation of the retention times and of ranged 80-94%. areas were 0.16 and 1.29%, respectively. Recoveries of the acetamiprid were in the analysis The proposed method is rapid, simple and could be utilized for the routine of acetamiprid residues in sweet cherry samples. PB - SZAB Kémiai Szakbizottsag Analitikai és Koernyezetvédelmi Munkabizottsaga C3 - Proceedings, 19th International Symposium on Analytical and Environmental Problems, 23 September 2013, Szeged, Hungary T1 - Determination of acetamiprid residues in sweet cherry samples. EP - 59 SP - 56 UR - https://hdl.handle.net/21.15107/rcub_fiver_3303 ER -
@conference{ author = "Lazić, Sanja and Šunjka, Dragana and Grahovac, Nada and Guzsvany, Valéria", year = "2013", abstract = "In this paper we have developed an analytical method for the fast determination of acetamiprid residue in sweet cherry samples. The experiment was carried out using blank extracted spiked with a solution of acetamipid insecticide at three levels. This analyte was preparation with acetonitrile from fortified sweet cherry samples using QUEChERS sample HPLC/DAD procedure. Insecticide determination and quantification were performed by x 4.6 mm using reversed phase procedure utilized an Agilent Zorbax Cj cartridge (50 mm internal diameter. 1.8 lum particle size). Mobile phase was acetonitrile/1.5% correlation CH3COOH solution. Acetamiprid showed linear calibrations from 0.05—2.5 ug/ml with mg/kg. coefficients of 0.995%. Limit of quantification (LOQ) were established as 0.014 the peak Precision values expressed as relative standard deviation of the retention times and of ranged 80-94%. areas were 0.16 and 1.29%, respectively. Recoveries of the acetamiprid were in the analysis The proposed method is rapid, simple and could be utilized for the routine of acetamiprid residues in sweet cherry samples.", publisher = "SZAB Kémiai Szakbizottsag Analitikai és Koernyezetvédelmi Munkabizottsaga", journal = "Proceedings, 19th International Symposium on Analytical and Environmental Problems, 23 September 2013, Szeged, Hungary", title = "Determination of acetamiprid residues in sweet cherry samples.", pages = "59-56", url = "https://hdl.handle.net/21.15107/rcub_fiver_3303" }
Lazić, S., Šunjka, D., Grahovac, N.,& Guzsvany, V.. (2013). Determination of acetamiprid residues in sweet cherry samples.. in Proceedings, 19th International Symposium on Analytical and Environmental Problems, 23 September 2013, Szeged, Hungary SZAB Kémiai Szakbizottsag Analitikai és Koernyezetvédelmi Munkabizottsaga., 56-59. https://hdl.handle.net/21.15107/rcub_fiver_3303
Lazić S, Šunjka D, Grahovac N, Guzsvany V. Determination of acetamiprid residues in sweet cherry samples.. in Proceedings, 19th International Symposium on Analytical and Environmental Problems, 23 September 2013, Szeged, Hungary. 2013;:56-59. https://hdl.handle.net/21.15107/rcub_fiver_3303 .
Lazić, Sanja, Šunjka, Dragana, Grahovac, Nada, Guzsvany, Valéria, "Determination of acetamiprid residues in sweet cherry samples." in Proceedings, 19th International Symposium on Analytical and Environmental Problems, 23 September 2013, Szeged, Hungary (2013):56-59, https://hdl.handle.net/21.15107/rcub_fiver_3303 .