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LC-MS/MS Determination of Tropane Alkaloids in Maize Crop
dc.creator | Vuković, Gorica | |
dc.creator | Bursić, Vojislava | |
dc.creator | Stojanović, Tijana | |
dc.creator | Petrović, Aleksandra | |
dc.creator | Gvozdenac, Sonja | |
dc.creator | Starović, Mira | |
dc.creator | Kuzmanović, Slobodan | |
dc.creator | Aleksić, Goran | |
dc.date.accessioned | 2021-04-26T19:42:33Z | |
dc.date.available | 2021-04-26T19:42:33Z | |
dc.date.issued | 2018 | |
dc.identifier.issn | 0350-1205 | |
dc.identifier.uri | http://fiver.ifvcns.rs/handle/123456789/1831 | |
dc.description.abstract | The undemanding LC-MS/MS method was developed for the synchronized analysis of atropine and scopolamine in maize crop. The dSPE was carried out with 1% acetic acid in acetonitrile/water and a mixture of magnesium sulphate, sodium chloride and sodium citrate. The analytes were separated on a Zorbax XDB C18 column using methanol/water as the mobile phase in gradient mode. The detection was done using a tandem masss spectrometry (MS/MS) in the positive ESI. The tropane alkaloids exhibited excellent linearity in the range of 2-20 µg/kg with the LOQ of 5 µg/kg for maize. The extraction recoveries of atropine and scopolamine were 65.7 and 85.5% with the intraday RSDr 10.25 and 4.29%, respectively. The validated method was appled to real maze samples. One sample contained 18.8 µg/kg of atropine and 6.3 µg/kg of scopolamine. | en |
dc.publisher | Novi Sad : Univerzitet u Novom Sadu - Poljoprivredni fakultet | |
dc.publisher | Novi Sad : Naučni institut za ratarstvo i povrtarstvo | |
dc.relation | info:eu-repo/grantAgreement/MESTD/Technological Development (TD or TR)/31018/RS// | |
dc.rights | openAccess | |
dc.rights.uri | https://creativecommons.org/licenses/by-nc-nd/4.0/ | |
dc.source | Savremena poljoprivreda | |
dc.subject | atropine | |
dc.subject | scopolamine | |
dc.subject | maize | |
dc.title | LC-MS/MS Determination of Tropane Alkaloids in Maize Crop | en |
dc.type | article | |
dc.rights.license | BY-NC-ND | |
dc.citation.epage | 226 | |
dc.citation.issue | 3-4 | |
dc.citation.other | 67(3-4): 221-226 | |
dc.citation.rank | M51 | |
dc.citation.spage | 221 | |
dc.citation.volume | 67 | |
dc.identifier.doi | 10.1515/contagri-2018-0032 | |
dc.type.version | publishedVersion |